CONTRIBUTORS .................................................. xii
Introduction: Goals and Challenges for the In-situ
Characterization of Heterogeneous Catalysts .................. 1
Jose A. Rodriguez, Jonathan C. Hanson, and Peter J. Chupas
1 QEXAFS in Catalysis Research: Principles, Data Analysis,
and Applications ............................................ 23
Anatoly I. Frenkel, Syed Khalid, Jonathan C. Hanson, and
Maarten Nachtegaal
2 Spatially Resolved X-ray Absorption Spectroscopy ............ 49
Christian G. Schroer and Jan-Dierk Grunwaldt
3 Energy-Dispersive EXAFS: Principles and Application in
Heterogeneous Catalysis ..................................... 75
Mark A. Newton and Andrew J. Dent
4 In-situ Powder X-ray Diffraction in Heterogeneous
Catalysis .................................................. 121
Jonathan Hanson and Poul Norby
5 Pair Distribution Function Analysis of High-Energy X-ray
Scattering Data ............................................ 147
Karena W. Chapman and Peter J. Chupas
6 Neutron Scattering for In-situ Characterization of
Heterogeneous Catalysis .................................... 169
Ashfia Huq and Wei-Ren Chen
7 Visualization of Surface Structures of Heterogeneous
Catalysts under Reaction Conditions or during Catalysis
with High-Pressure Scanning Tunneling Microscopy ........... 191
Luan Nguyen, Shiran Zhang, Yingchun Ye, Yuan Zhu, Lei
Wang, and Franklin (Feng) Tao
8 In-situ Infrared Spectroscopy on Model Catalysts ........... 209
Kumudu Mudiyanselage and Dario J. Stacchiola
9 Infrared Spectroscopy on Powder Catalysts .................. 241
Eli Stavitski
10 Structural Characterization of Catalysts by Operando
Raman Spectroscopy ......................................... 267
Gerhard Mestl and Miguel A. Bañares
11 In-situ Electron Paramagnetic Resonance of Powder
Catalysts .................................................. 293
Angelika Brückner
12 Application of Ambient-Pressure X-ray Photoelectron
Spectroscopy for the In-situ Investigation of
Heterogeneous Catalytic Reactions .......................... 315
David E. Starr, Hendrik Bluhm, Zhi Liu, Axel Knop-
Gericke, and Michael Hävecker
13 Combined X-ray Diffraction and Absorption Spectroscopy
in Catalysis Research: Techniques and Applications ......... 345
Anatoly I. Frenkel and Jonathan C. Hanson
14 Combining Infrared Spectroscopy with X-ray Techniques
for Interrogating Heterogeneous Catalysts .................. 369
Mark A. Newton and Marcos Fernández-Garcáa
15 XRD-Raman and Modulation Excitation Spectroscopy ........... 411
Wouter van Beek, Atsushi Urakawa, and Marco Milanesio
16 Catalyst Imaging Using Synchrotron-Based Multitechnique
Approaches ................................................. 441
Andrew M. Beale, Javier Ruiz-Martinez, and Bert
M. Weckhuysen
INDEX ......................................................... 475
|
