Contributors .................................................. vii
Preface ........................................................ ix
1 Recent Advances of Solid-State NMR Studies on Zeolites ....... 1
Shenhui Li and Feng Deng
1 Introduction .............................................. 2
2 Topology Structure of Zeolites ............................ 3
3 Crystallization Mechanism of Zeolites ..................... 8
4 Host-Guest Interactions in Zeolites ...................... 14
5 Active Sites in Zeolites ................................. 18
6 Reaction Mechanism Elucidation from In Situ NMR .......... 36
7 Conclusion and Outlook ................................... 43
Acknowledgements ............................................ 44
References .................................................. 44
2 Applications of Projection NMR Techniques ................... 55
Torsten Herrmann and Benedicte Elena-Herrmann
1 Introduction ............................................. 56
2 Principles of Projection NMR Spectroscopy ................ 57
3 Applications of Projection Spectroscopy to Biomolecular
NMR ...................................................... 68
4 Applications to Solution NMR of Small Organic Molecules
and Metabolic Profiling Investigations ................... 86
5 Applications of Projections to High-Resolution Solid-
State NMR Spectroscopy of Materials ...................... 89
6 Conclusions .............................................. 96
References .................................................. 97
3 Optical Atomic Magnetometry for Ultra-Low-Field
NMR Detection .............................................. 103
G. Bevilacqua, V. Biancalana, Y. Dancheva, and L. Moi
1 Introduction ............................................ 104
2 Generalities of OAMs .................................... 111
3 Constructive and Operative Details of a Selected OAM .... 116
4 Detection of Proton Precession .......................... 123
5 Microtesla MRI .......................................... 131
6 Zero- and Near-Zero-Field NMR with Labelled Molecules:
Proton, 13CJ-J Coupling .................................. 134
7 Improving the Signal-to-Noise Ratio in ULF-NMR: Merged
Samples and Hyperpolarization Experiments ............... 138
8 Conclusion .............................................. 140
References ................................................. 140
4 NMR Studies of Molten Salt and Room Temperature Ionic
Liquids .................................................... 149
Anne-Laure Rollet and Catherine Bessada
1 Introduction ............................................ 150
2 Molten Salts ............................................ 151
3 Room Temperature Ionic Liquids .......................... 169
4 Conclusion .............................................. 199
Acknowledgements ........................................... 200
References ................................................. 200
5 Intermolecular Zero Quantum Coherence in NMR
Spectroscopy ............................................... 209
Yulan Lin, Yuqing Huang, Shuhui Cai, and Zhong Chen
1 Introduction ............................................ 210
2 Theoretical Frame for iZQC Signals ...................... 213
3 ID High-Resolution iZQC Spectroscopic Techniques ........ 223
4 2D High-Resolution iZQC Spectroscopic Techniques ........ 242
5 In Vivo Application of iZQC Spectroscopic Techniques .... 247
6 Conclusion .............................................. 253
Acknowledgements .............................................. 253
References .................................................... 253
Index ......................................................... 259
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