Annual reports on NMR spectroscopy. Vol.70 / ed. by G.A.Webb. - Oxford: Academic Press, 2010. - ix, 247 p.: ill. - Incl. bibl. ref. - Sub. ind.: p.241-247. - ISBN 978-0-12-381353-4  Место хранения:   032 | Институт органической химии им. Н.Н.Ворожцова СО РАН | Новосибирск | Библиотека

Оглавление / Contents

Contributors .................................................. vii Preface ........................................................ ix 1 Recent Developments in Liquid-State INADEQUATE Studies ....... 1 Dušan Uhrín 1 Introduction .............................................. 2 2 INADEQUATE-The Basic Concept .............................. 3 3 Increasing the Sensitivity of INADEQUATE .................. 4 4 Measurement of 13C-13C Coupling Constants ................. 14 5 Applications of High-Resolution INADEQUATE to 13C ........ 19 6 Applications of INADEQUATE to Nuclei Other Than 13C ...... 26 7 Outlook .................................................. 32 References .................................................. 32 2 Phosphorus-31 NMR Spectroscopy of Condensed Matter .......... 35 Marek J. Potrzebowski, Sławomir Kaźmierski, Hassan Kassassir, and Beata Miksa 1 Introduction ............................................. 36 2 Progress in Methodology .................................. 37 3 Applications of 13P SS NMR Spectroscopy .................. 55 4 Concluding Remarks ...................................... 107 Acknowledgement ............................................ 107 References ................................................. 107 3 Recent Applications of Solid-State 170 NMR ................. 115 K. Yamada 1 Introduction ............................................ 116 2 17O Synthesis ........................................... 118 3 Background of Solid-State 17O NMR ....................... 120 4 Fundamentals of 17O NMR in Biological Solids ............ 127 5 Applications of Solid-State 17O NMR in Biochemistry ..... 148 6 Conclusions ............................................. 155 References ................................................. 156 4 Spatial Inhomogeneity of Cavities in Polymer Network Systems as Characterised by Field-Gradient NMR Using Probe Diffusant Molecules and Polymers with Different Sizes ...................................................... 159 Kazuhiro Kamiguchi, Shigeki Kuroki, Yuji Yamane, Mitsuru Satoh, and Isao Ando 1 Intro'duction ........................................... 160 2 Network Structure of Polymer Gels and Diffusional Behaviour of Probe Polymers ............................. 161 3 Network Structure of Micrometre-Scale Cavity Obtained from Phase-Separated Polymer Blends as Characterised by Using Probe Molecules ................................ 192 4 Conclusions ............................................. 199 References ................................................. 199 5 Practical NMR Analysis of Morphology and Structure of Polymers ................................................... 203 Takeshi Yamanobe, Hiroki Uehara, and Masaki Kakiage 1 Introduction ............................................ 204 2 Analysis Method of Free Induction Decay of Pulse NMR for Polymers ............................................ 206 3 Morphology and Relaxation Behaviour ..................... 210 4 Kinetics of Dynamic Process of Polymers ................. 229 5 Conclusions ............................................. 238 References ................................................. 238 Subject Index ................................................. 241