Preface ....................................................... iii
Contributors ................................................... xi
1. A Perspective on Zeolite Synthesis: How Do You Know
What You'll Get? ............................................. 1
M.E. Davis and S.I. Zones
2. Influence of Physicochemical and Structural Properties of
Aluminosilicate Gel Precursors on the Kinetics of
Crystallization Zeolites A and X ............................ 35
B. Subotic, T. Antonic, I. Smit, R. Aiello, F. Crea,
A. Nastro, and F. Testa
3. Homogeneous Versus Heterogeneous Zeolite Nucleation.
A SAXS-WAXS Study ........................................... 59
Theo P. M. Beelen, Wim H. Dokter, Harold F. van
Garderen, and Rutger A. van Santen
4. Synthesis and Characterization of UTD-1: A Novel Zeolite
Molecular Sieve ............................................. 77
K.J. Balkus, Jr., A.G. Gabrielov, S.I. Zones,
and I.Y. Chan
5. The Synthesis of Omega Zeolite From a TMA-Free System
Which Uses p-dioxane as a Co-Solvent ........................ 93
S.I. Zones
6. The Structure Directing Effect of Fluoride in the AI2O3-
P2O5-HF-TEAOH-H2O System ................................... 115
Erling Halvorsen, Arne Karlsson, Duncan Akporiaye,
and Karl Petter Lillerud
7. Factors Affecting the MTW Zeolite Crystallization
Process .................................................... 127
Andrea Katovic and Girolamo Giordano
8. The Deposition of Zeolites from the Gas Phase .............. 139
R. Althoff, B. Sellegreen, B. Zibrowius, K. Unger,
and F. Schüth
9. Stable Suspensions of Colloidal Silicalite-1 Crystals
Free from Organic Material ................................. 159
Anders E. Persson, Brian J. Schoeman, Johan Sterte,
and Jan-Erik Otterstedt
10.Semi-batch Synthesis of Silicalite-1 from Alkaline
Aqueous Solutions by Monitored Addition of an Acid or
an Alcohol ................................................. 175
P.Y. Le Goff, P. Caullet, J.L. Guth, and E. Benazzi
11.Flux Growth of Millimeter-Sized Single Crystal
Aluminate Sodalite ......................................... 189
T. Okubo, J. Sun, C.B. Dartt, and M.E. Davis
12.Synthesis of Aluminophosphates in the Presence of Metal-
Chelate Complexes .......................................... 197
Stefan Ernst
13.Synthesis of Octahedral Molecular Sieves and Layered
Materials .................................................. 215
Steven L. Suib and Chi-Lin О Young
14.Preparation of Two Cobalt-Substituted Zincophosphate
Molecular Sieves ........................................... 233
Nevenka Rajic, Natasa Zabukovec Logar, Anton Meden,
and Venceslav Kaucic
15.Synthesis of VPI-8: The First Large Pore Zincosilicate ..... 243
M.A. Camblor, M. Yoshikawa, S.I. Zones, and M.E. Davis
16.Template Directed Synthesis of the High-Silica
Microporous Materials RUB-3, RUB-4, RUB-10 and RUB-13 ...... 263
B. Marler, U. Oberhagemann, S. Vortmann,
A. Grünewald-Luke, and H. Gies
17.Synthesis and Characterization of Several Gallium-
Containing Molecular Sieves with the Offretite Structure ... 283
Mario L. Occelli, H. Eckert, P.S. Iyer, and P. Ritz
18.Synthesis and Characterization of Ga-substituted Zeolite
ZSM-20 ..................................................... 299
H. Kosslick, V. A. Tuan, G Walther, H. Miessner,
R. Fricke, and W. Storek
19.Ferrierite: As Synthesized and Dealuminated with a Si/Al
Ratio From 10 to Infinity .................................. 315
Kristin Vinje, Conrad Ingram, Rosemarie Szostak, and
Karl Fetter Lillerud
20.Kilogram Scale Production of EMT Zeolite: Optimization
of the Synthesis Conditions ................................ 325
D. Anglerot, F. Fitoussi, Ph. Schulz, T. Chatelain,
F. Dougnier, J. Patarin, and J.L. Guth
21.The Kinetics of Solid-State Ion Exchange Between CuCl
and Sodium Forms of Zeolites ............................... 335
Ming Jiang, Jtirgen Koy, and Hellmut G. Karge
22.Heteropolytungstates with Cavities: the Influence of
the Template on the Structure .............................. 345
M. Holscher, A. Gammersbach, B. Zibrowius,
U. Englert, and W.F. Holderich
23.The Synthesis and Reactivity of Zeolite NaX
Encapsulated Ruthenium Perfluorophthalocyanines ............ 363
Kenneth J. Balkus, Jr., Mona Eissa, and Rosario
Lavado
24.Self-Assembly of Silicate-Surfactant Liquid Crystals
During Mesophase Materials Synthesis ....................... 379
A. Firouzi, G.D. Stucky, and B.F. Chmelka
25.A Simple Geometric Modelling of the Porosity of MCM-41
Type Materials ............................................. 391
G. Schulz-Ekloff, J. Rathousky, and A. Zukal
26.Ti-Modified Mesoporous Molecular Sieves, Ti-MCM-41
and Ti-MHS ................................................. 405
J. Sudhakar Reddy, Awa Dicko, and Abdelhamid Sayari
27.Synthesis and Spectroscopic Studies of Vanadium-
Containing Molecular Sieves ................................ 417
A. Sayari, I.L. Moudrakovski, C.I. Ratcliffe,
J.A. Ripmeester, and K.F. Preston
28.Preparation and Characterization of Acidic Properties
of MCM-41 .................................................. 431
Ramesh B. Borade and Abraham Clearfield
29.The Synthesis of Hectorite: A Template Effect? ............. 451
K.Y. Jacobs, J. Soers, and R.A. Schoonheydt
30.Synthesis of Dioctahedral 2:1 Layer Silicates in an Acid
and Fluoride Medium ........................................ 465
Laurent Huve, Ronan Le Dred, Daniel Saehr, and
Jacques Baron
31.On the Structural Stability of Smectites Pillared with
Al and Al-La Polyoxocations ................................ 491
L. Caballero, J. M. Dominguez, J. L. De Los Santos,
A. Montoya, and J. Navarrete
32.Silica-pillared Layered Metal(IV) Phosphates ............... 509
Thierry Cassagneau, Deborah J. Jones, Pedro Maireles-
Torres, and Jacques Roziere
33.Improvement of the Pillaring Process for Synthetic and
Natural Beidellite ......................................... 523
Jocelyne Miehe, Ronan Le Dred, Jacques Baron, and
Daniel Saehr
34.Determination of the Pillar Structure in Chromia-
Pillared Layered Phosphates Using X-Ray Absorption
Spectroscopy ............................................... 537
Deborah J. Jones, Jacques Roziere, Pedro Maireles-
Torres, Antonio Jimenez-Lopez, Pascual Olivera-
Pastor, Enrique Rodriguez-Castellon, and Anthony
A.G. Tomlinson
35.Porous Networks Derived From Synthetic Polymer-Clay
Complexes .................................................. 551
Kathleen A. Carrado, P. Thiyagarajan, and Delwin
L. Elder
36.Synthesis, Modification, and Catalytic Properties of
Layered Silicates: Kanemite and Magadiite .................. 567
E. Terres-Rojas, J.M. Dominguez, M.A. Leyva,
R.P. Salas, and E. Lopez
37.Fatty Acid Chains in Lithium Aluminum Layered Double
Hydroxides: A New Class of Gas Chromatographic
Stationary Phase ........................................... 595
Michael Jakupca and Prabir K. Dutta
38.Post-Synthesis Modification of Layered Double
Hydroxides ................................................. 607
C. Forano, A. de Roy, C. Depege, M. Khaldi,
F.Z. El Metoui, and J.P. Besse
39.Intercalation of Porphyrin in Zn-Al Layered Double
Hydroxides ................................................. 627
S. Bonnet, L. Bigey, С. Forano, A. de Roy,
J.P. Besse, P. Maillard, and M. Momenteau
40.The Incorporation of Benzoate and Terephthalate Anions
into Layered Double Hydroxides ............................. 641
F. Kooli and W. Jones
41.Layered Hydroxycarbonates with the Hydrotalcite
Structure Containing Zn, Al, and Fe ........................ 661
C. Barriga, F. Kooli, V. Rives, and M.A. Ulibarri
42.Reactions of Hydrotalcite-like Compounds with Silicates
and Phosphates ............................................. 675
Verena Seefeld, Wolfgang Gessner, Ulrich Schulke,
and Dirk Miiller
43.Synthesis of Hydrotalcite-Like Materials with a Sheet-
Like Morphology ............................................ 691
С.P. Kelkar, A.A. Schutz, and L.A. Cullo
Index ......................................................... 705
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