List of Contributors ............................................ v
Preface ....................................................... vii
Long-Range 1H-15N Heteronuclear Shift Correlation
GARY E. MARTIN AND ANTONY J. WILLIAMS
1. Introduction ................................................. 2
2. New Long-Range Heteronuclear Shift Correlation Methods ....... 2
3. NMR Probe Technology Developments ........................... 10
4. Computer-Assisted Structure Elucidation Using 15N Chemical
Shift and 1H-15N Long-Range Correlation Information .......... 12
5. Long-Range Correlation Studies Involving 15N ................. 24
6. Conclusions ................................................ 113
References .................................................... 113
Magic-Angle-Spinning Solid-State NMR Applied to Polypeptides
and Proteins
COLAN E. HUGHES AND MARC BALDUS
1. Introduction ............................................... 121
2. Methods .................................................... 123
3. Applications ............................................... 142
4. Conclusions ................................................ 152
Acknowledgements .............................................. 153
References .................................................... 153
NMR Studies of Dynamic Processes in Organic Solids
D. REICHERT
1. Introduction ............................................... 159
2. Experimental Methods ....................................... 161
3. Applications of Dynamic Solid-State NMR in Organic
Solids ..................................................... 179
4. Conclusions ................................................ 188
References .................................................... 188
NMR Studies of Nanoparticles
CHRISTIAN MAYER
1. Introduction ............................................... 205
2. Nuclear Magnetic Resonance Techniques ...................... 206
3. Numerical Simulation Procedure ............................. 209
4. General Applications and Examples .......................... 220
5. Conclusion ................................................. 256
References .................................................... 257
Microscopy in Magnetic Resonance Imaging
P.T. NARASIMHAN AND RUSSELL E. JACOBS
1. Introduction ............................................... 260
2. Signal and Noise in Magnetic Resonance Imaging ............. 261
3. Contrast ................................................... 263
4. Imaging Methods, Pulse Sequences, and the Point Spread
Function ................................................... 270
5. Other Imaging Methods ...................................... 273
6. Applications ............................................... 275
7. Prospects for Higher Resolution ............................ 287
Acknowledgements .............................................. 289
References .................................................... 289
Applications of Optical Pumping and Polarization Techniques in NMR:
I. Optical Nuclear Polarization in Molecular Crystals
BOYD M. GOODSON
1. Introduction ............................................... 300
2. ONP in Molecular Crystals .................................. 303
Acknowledgements .............................................. 320
References .................................................... 321
Index ......................................................... 325
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