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ОбложкаMonitoring polymerization reactions: from fundamentals to applications / ed.: W.F.Reed, A.M.Alb. - Hoboken: Wiley, 2014. - xiv, 473 p.: ill. + 6 p. ill. - Bibliogr. at the end of the chapters. - Ind.: p.451-473.1 - ISBN 978-0-470-91738-1
Шифр: (И/Г7-M81) 02
 

Место хранения: 02 | Отделение ГПНТБ СО РАН | Новосибирск

Оглавление / Contents
 
PREFACE ........................................................ ix
INTRODUCTION ................................................... xi
CONTRIBUTORS ................................................. xiii

SECTION I  OVERVIEW OF POLYMERIZATION REACTIONS AND KINETICS .... 1
1  Free Radical and Condensation Polymerizations ................ 3
   Matthew Kade and Matthew Tirrell
2  Overview of Controlled/Living Polymerization Methods of
   Vinyl Monomers .............................................. 29
   Robert T. Mathers, Andrew J. D. Magenau, Kristin Schröder,
   and Krzysztof Matyjaszewski
3  Stimuli-Responsive Polymers via Controlled Radical
   Polymerization .............................................. 45
   Joel D. Flores, Brooks A. Abel, DeeDee Smith, and Charles
   L. McCormick
4  Reactions in Heterogeneous Media: Emulsion, Miniemulsion,
   Microemulsion, Suspension, and Dispersion Polymerization .... 59
   Radmila Tomovska, José C. de la Cal, and José M. Asua

SECTION 2  POLYMERIZATION CHARACTERIZATION AND MONITORING
METHODS ........................................................ 79
5  Polymer Characteristics ..................................... 81
   Wayne F. Reed
6  Infrared (MIR, NIR), Raman, and Other Spectroscopic
   Methods .................................................... 107
   Alexandre F. Santos, Fabricio M. Silva, Marcelo К. Lenzi,
   and Jose С. Pinto
7  Calorimetry, Conductivity, Densimetry, and Rheological
   Measurements ............................................... 135
   Jose R. Leiza and Timothy McKenna
8  Light Scattering ........................................... 151
   Guy C. Berry
9  GPC/SEC as a Key Tool for Assessment of Polymer Quality
   and Determination of Macromolecular Properties ............. 171
   Daniela Held and Peter Kilz
10 Mass Spectroscopy: ESR and NMR Applications to Polymer
   Characterization and Polymerization Monitoring ............. 201
   Zifu Zhu and Alina M. Alb

SECTION 3  AUTOMATIC CONTINUOUS ONLINE MONITORING
OF POLYMERIZATION REACTIONS (ACOMP) ........................... 229
11 Background and Principles of Automatic Continuous Online
   Monitoring of Polymerization Reactions (ACOMP) ............. 231
   Wayne F. Reed
12 Applications of ACOMP (I) .................................. 247
   Alina M. Alb
13 Applications of ACOMP (II) ................................. 271
   Wayne F. Reed
14 Cognate Techniques to ACOMP ................................ 295
   Michael F. Drenski, Alina M. Alb, and Wayne F. Reed
15 Outlook for Industrial ACOMP ............................... 313
   Michael F. Drenski and Alex W. Reed

SECTION 4  REACTOR CONTROL AND DESIGN: BATCH, SEMI-BATCH,
AND CONTINUOUS REACTORS ....................................... 325
16 Mathematical Modeling of Polymerization Reactors ........... 327
   F. Joseph Schork
17 Design and Operation of Polymerization Reactors ............ 345
   F. Joseph Schork
18 Optimization of the Particle Size in Emulsion
   Polymerization ............................................. 363
   Joseph Zeaiter and José A. Romagnoli

SECTION 5  INDUSTRIAL APPLICATIONS ............................ 381
19 Water-Soluble Free Radical Addition Polymerizations ........ 383
   Wesley L. Whipple and Hua Zheng
20 Protein Aggregation in Pharmaceutical Biotechnology ........ 395
   Mark L. Brader
21 Rubbers and Elastomers ..................................... 409
   Jorge Soto
22 Polymers from Natural Products ............................. 427
   Dimitrios Samios, Aline Nicolau, and Miriam B. Roza

Index ......................................................... 451

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